Material Strength Analysis of Glazes Derived from Soda Lime Cullet on Ceramic Tiles

Razaq Olatunde Rom Kalilu

Department of Fine and Applied Arts, Faculty of Environmental Sciences, Ladoke Akintola University of Technology, Ogbomoso, Nigeria.

Michael Olaniyi Ajadi *

Department of Fine and Applied Arts, Faculty of Environmental Sciences, Ladoke Akintola University of Technology, Ogbomoso, Nigeria.

*Author to whom correspondence should be addressed.


Abstract

Strength analysis is a mechanical reliability assessment used to determine the probability of material failure and to establish whether applied stress exceeds material strength. This study evaluated the strength and strain characteristics of studio-produced glazes derived from soda-lime cullet and applied to ceramic tiles. Beverage glass bottles and windowpane glass were collected from waste dumps, garbage cans and construction sites, washed, heated at 120 °C to remove residual oily stains, pulverised and sieved to obtain compatible particle-size densities for glaze preparation. Particle-size density determined by the Blaine method was 2280 kg/m³ for the cullet samples and clay, and 3110 kg/m³ for borax, soda ash and potash. Oxide properties were examined using the Particle-Induced X-ray Emission technique. Glaze batches were formulated by milling the cullet with ball clay and selected fluxes, namely borax, soda ash and potash, before application to biscuit-fired ceramic tiles and glaze firing at 950 °C. Mechanical performance was assessed using a digital universal testing machine under compressive loading. The oxide analysis showed that the cullet samples contained 63.73-78.30% SiO2, 12.81-13.85% Na2O, 4.94-7.16% CaO and 0.67-3.37% MgO. Windowpane cullet produced more melt-glossy outputs than beverage cullet. Among the glaze recipes, WtwCB and WblCB showed the highest resistance to break, with compressive strength/strain values of 1.16162 MPa/0.15608 mm/mm and 1.26268 MPa/0.22542 mm/mm, and Young’s modulus values of 14.653498 N/mm² and 15.550096 N/mm², respectively. The results indicate that selected soda-lime cullet compositions, when combined with appropriate fluxes, can produce visually acceptable and mechanically resistant glazes for ceramic tiles.

Keywords: Cullet, soda-lime glass, ceramic tiles, glass-ceramic glaze, oxide properties, PIXE, compressive strength, compressive strain, Young’s modulus, glaze firing, waste glass recycling


How to Cite

Kalilu, Razaq Olatunde Rom, and Michael Olaniyi Ajadi. 2026. “Material Strength Analysis of Glazes Derived from Soda Lime Cullet on Ceramic Tiles ”. Advances in Research 27 (4):377-90. https://doi.org/10.9734/air/2026/v27i41679.

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